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Amino acid compound specific isotope values for particles from R/V Kilo Moana KM1407 and KM1418 in the Central North Pacific, Station ALOHA, Tropical Pacific, Feb and Sept. 2014 (NCEI Accession 0278030)

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This dataset contains chemical data collected on R/V Kilo Moana during cruises KM1407 and KM1418 from 2014-02-19 to 2014-09-11. These data include d15N and depth. The instruments used to collect these data include Gas Chromatograph, Ion Chromatograph, and Large Volume Pumping System-WTS-LV. These data were collected by Dr Brian N. Popp, Dr Cecelia Hannides, Dr Jeffrey C. Drazen, and Dr Kanesa Seraphin of University of Hawaii at Manoa, Dr Joel Blum of University of Michigan Ann Arbor, and Dr Claudia Benitez-Nelson of University of South Carolina at Columbia as part of the "Collaborative Research: Isotopic insights to mercury in marine food webs and how it varies with ocean biogeochemistry (Hg_Biogeochemistry)" project. The Biological and Chemical Oceanography Data Management Office (BCO-DMO) submitted these data to NCEI on 2019-03-18.

The following is the text of the dataset description provided by BCO-DMO:

Amino acid specific isotopes in particles, station ALOHA

Dataset Description:
This dataset contains amino acid compound specific nitrogen isotope ratios in particles collected during R/V Kilo Moana cruises around Station ALOHA (KM1407 and KM1418).

For more information about the ALOHA observatory see: http://aco-ssds.soest.hawaii.edu/

These data were published in Gloeckler et al (2018), Supporting Information file lno10762-sup-0002-suppinfo2.xlsx

Dataset Citation

Cite as: Popp, Brian N.; Benitez-Nelson, Claudia R.; Blum, Joel D.; Drazen, Jeffrey C.; Hannides, Cecelia; Seraphin, Kanesa (2023). Amino acid compound specific isotope values for particles from R/V Kilo Moana KM1407 and KM1418 in the Central North Pacific, Station ALOHA, Tropical Pacific, Feb and Sept. 2014 (NCEI Accession 0278030). [indicate subset used]. NOAA National Centers for Environmental Information. Dataset. https://www.ncei.noaa.gov/archive/accession/0278030. Accessed [date].

Dataset Identifiers

ISO 19115-2 Metadata

gov.noaa.nodc:0278030

Full Text · XML

Download Data	HTTPS (download) Navigate directly to the URL for data access and direct download. FTP (download) These data are available through the File Transfer Protocol (FTP). FTP is no longer supported by most internet browsers. You may copy and paste the FTP link to the data into an FTP client (e.g., FileZilla or WinSCP).
Distribution Formats	TSV
Ordering Instructions	Contact NCEI for other distribution options and instructions.
Distributor	NOAA National Centers for Environmental Information +1-301-713-3277 NCEI.Info@noaa.gov
Dataset Point of Contact	NOAA National Centers for Environmental Information ncei.info@noaa.gov

Time Period	2014-02-19 to 2014-09-11
Spatial Bounding Box Coordinates	West: -158 East: -158 South: 22.75 North: 22.75
Spatial Coverage Map

General Documentation

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Descriptive Information
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Associated Resources

Biological, chemical, physical, biogeochemical, ecological, environmental and other data collected from around the world during historical and contemporary periods of biological and chemical oceanographic exploration and research managed and submitted by the Biological and Chemical Oceanography Data Management Office (BCO-DMO)
- NCEI Collection
  Navigate directly to the URL for data access and direct download.
Popp, B., Hannides, C., Drazen, J., Seraphin, K., Blum, J., Benitez-Nelson, C. (2018) Amino acid compound specific isotope values for particles from R/V Kilo Moana KM1407 and KM1418 in the Central North Pacific, Station ALOHA, Tropical Pacific, Feb and Sept. 2014. Biological and Chemical Oceanography Data Management Office (BCO-DMO). Dataset version 2018-12-05. https://doi.org/10.1575/1912/bco-dmo.751313.1
- https://doi.org/10.1575/1912/bco-dmo.751313.1 (download)
  originator dataset

gov.noaa.nodc:BCO-DMO

Publication Dates	publication: 2023-05-11
Data Presentation Form	Digital table - digital representation of facts or figures systematically displayed, especially in columns
Dataset Progress Status	Complete - production of the data has been completed Historical archive - data has been stored in an offline storage facility
Data Update Frequency	As needed
Supplemental Information	Acquisition Description: Amino acid-specific stable N isotope composition was determined on samples that were hydrolyzed, derivatized, and analyzed according to Popp et al. (2007) and Hannides et al. (2009). Briefly, size-fractioned zooplankton material and target zooplankton taxa were hydrolyzed using trace metal-grade 6 M HCl and the resulting AAs purified using cation exchange chromatography. The samples were then esterified using 4:1 isopropanol:acetyl chloride and derivatized using 3:1 methylene chloride:trifluoroacetyl anhydride. The resulting trifluoroacetyl and isopropyl ester (TFA) derivatives were purified using chloroform extraction and stored at -20°C for up to 1 month before analysis. This method yielded information for the following AAs: alanine (Ala), glycine (Gly), isoleucine (Ile), leucine (Leu), lysine (Lys), methionine (Met), phenylalanine (Phe), proline (Pro), serine (Ser), threonine (Thr), tyrosine (Tyr), and valine (Val). During acid hydrolysis asparagine (Asn) is converted to aspartic acid (Asp) and glutamine (Gln) is converted to glutamic acid (Glu), thus we also report information on the combined pools, termed Asx (Asn+Asp) and Glx (Gln+Glu), respectively. TFA derivatives of AAs were analyzed for stable N isotope composition (d15NAA values) following Hannides et al. (2013). AAs were analyzed using a Thermo Scientific Delta V Plus IRMS interfaced to a trace gas chromatograph (GC) fitted with a 60 m BPx5 capillary column through a GC-C III combustion furnace (980°C), reduction furnace (680°C) and liquid nitrogen cold trap. d15NAA values were measured on 3 – 5 replicate injections with norleucine and aminoadipic acid with known d15N values as internal reference materials co-injected on each run. A composite source d15NAA value was calculated by a weighted averaging a suite of AAs (e.g., d15NSrc-AA = average of Gly, Lys, Phe, and Ser d15N values). Weighting was based the analytical uncertainty calculated from at least triplicate analysis of each sample.
Purpose	This dataset is available to the public for a wide variety of uses including scientific research and analysis.
Use Limitations	accessLevel: Public Distribution liability: NOAA and NCEI make no warranty, expressed or implied, regarding these data, nor does the fact of distribution constitute such a warranty. NOAA and NCEI cannot assume liability for any damages caused by any errors or omissions in these data. If appropriate, NCEI can only certify that the data it distributes are an authentic copy of the records that were accepted for inclusion in the NCEI archives.

Dataset Citation	Cite as: Popp, Brian N.; Benitez-Nelson, Claudia R.; Blum, Joel D.; Drazen, Jeffrey C.; Hannides, Cecelia; Seraphin, Kanesa (2023). Amino acid compound specific isotope values for particles from R/V Kilo Moana KM1407 and KM1418 in the Central North Pacific, Station ALOHA, Tropical Pacific, Feb and Sept. 2014 (NCEI Accession 0278030). [indicate subset used]. NOAA National Centers for Environmental Information. Dataset. https://www.ncei.noaa.gov/archive/accession/0278030. Accessed [date].
Cited Authors	Popp, Brian N. University of Hawaii at Manoa Benitez-Nelson, Claudia R. University of South Carolina at Columbia Blum, Joel D. University of Michigan Ann Arbor Drazen, Jeffrey C. University of Hawaii at Manoa Hannides, Cecelia University of Hawaii at Manoa Seraphin, Kanesa University of Hawaii at Manoa
Principal Investigators	Brian N. Popp University of Hawai'i at Mānoa (UHM) Claudia R. Benitez-Nelson University of South Carolina (USC) Joel D. Blum University of Michigan Jeffrey C. Drazen University of Hawai'i at Mānoa (UHM) Cecelia Hannides University of Hawai'i at Mānoa (UHM) Kanesa Seraphin University of Hawai'i at Mānoa (UHM)
Contributors	University of South Carolina (USC) University of Hawai'i at Mānoa (UHM)
Resource Providers	Biological and Chemical Oceanography Data Management Office (BCO-DMO)
Points of Contact	Biological and Chemical Oceanography Data Management Office (BCO-DMO)
Publishers	NOAA National Centers for Environmental Information
Acknowledgments	Funding provided by NSF Division of Ocean Sciences (NSF OCE) Award Number: OCE-1433846 Award URL: http://www.nsf.gov/awardsearch/showAward.do?AwardNumber=1433846

Theme keywords	NODC DATA TYPES THESAURUS DELTA NITROGEN-15 DEPTH - OBSERVATION NODC OBSERVATION TYPES THESAURUS chemical WMO_CategoryCode oceanography BCO-DMO Standard Parameters comments d15N depth diameter sample identification Global Change Master Directory (GCMD) Science Keywords EARTH SCIENCE > OCEANS > OCEAN CHEMISTRY > NITROGEN Originator Parameter Names Depth Particle_size Sample comment delta15N delta15N_stdev
Data Center keywords	NODC COLLECTING INSTITUTION NAMES THESAURUS University of Hawai'i at Mānoa University of South Carolina NODC SUBMITTING INSTITUTION NAMES THESAURUS Biological and Chemical Oceanography Data Management Office Global Change Master Directory (GCMD) Data Center Keywords BCO-DMO > Biological and Chemical Oceanography Data Management Office
Platform keywords	NODC PLATFORM NAMES THESAURUS R/V KILO MOANA BCO-DMO Platform Names R/V Kilo Moana Global Change Master Directory (GCMD) Platform Keywords Ships ICES/SeaDataNet Ship Codes Kilo Moana (call sign: WDA7827, ICES code: 33KB, 2002)
Instrument keywords	NODC INSTRUMENT TYPES THESAURUS chromatograph BCO-DMO Standard Instruments Gas Chromatograph Ion Chromatograph Large Volume Pumping System-WTS-LV Global Change Master Directory (GCMD) Instrument Keywords GAS CHROMATOGRAPHS > GAS CHROMATOGRAPHS Originator Instrument Names Thermo Scientific Delta V Plus IRMS unknown (Ion Chromatograph) unknown (Large Volume Pumping System-WTS-LV)
Place keywords	Provider Place Names Central North Pacific, Station ALOHA
Project keywords	BCO-DMO Standard Projects Collaborative Research: Isotopic insights to mercury in marine food webs and how it varies with ocean biogeochemistry (Hg_Biogeochemistry) Provider Cruise IDs KM1407 KM1418 Provider Funding Award Information Funding provided by NSF Division of Ocean Sciences (NSF OCE) Award Number: OCE-1433846
Keywords	NCEI ACCESSION NUMBER 0278030

Use Constraints	Cite as: Popp, Brian N.; Benitez-Nelson, Claudia R.; Blum, Joel D.; Drazen, Jeffrey C.; Hannides, Cecelia; Seraphin, Kanesa (2023). Amino acid compound specific isotope values for particles from R/V Kilo Moana KM1407 and KM1418 in the Central North Pacific, Station ALOHA, Tropical Pacific, Feb and Sept. 2014 (NCEI Accession 0278030). [indicate subset used]. NOAA National Centers for Environmental Information. Dataset. https://www.ncei.noaa.gov/archive/accession/0278030. Accessed [date].
Data License	This dataset is licensed under a Creative Commons Attribution 4.0 International (CC BY 4.0) License. SPDX License: Creative Commons Attribution 4.0 International (CC-BY-4.0)
Access Constraints	Use liability: NOAA and NCEI cannot provide any warranty as to the accuracy, reliability, or completeness of furnished data. Users assume responsibility to determine the usability of these data. The user is responsible for the results of any application of this data for other than its intended purpose.
Fees	In most cases, electronic downloads of the data are free. However, fees may apply for custom orders, data certifications, copies of analog materials, and data distribution on physical media.

Lineage information for: dataset
Processing Steps	2023-05-11T05:01:03Z - NCEI Accession 0278030 v1.1 was published.
Output Datasets	NCEI Accession 0278030 v1.1 NCEI Accession 0278030 v1.1 (download) published 2023-05-11T05:01:03Z

Acquisition Information (collection)
Instrument	chromatograph
Platform	R/V KILO MOANA

Last Modified: 2024-06-26T18:45:28Z
For questions about the information on this page, please email: ncei.info@noaa.gov

Amino acid compound specific isotope values for particles from R/V Kilo Moana KM1407 and KM1418 in the Central North Pacific, Station ALOHA, Tropical Pacific, Feb and Sept. 2014 (NCEI Accession 0278030)

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