Sediment pore water and solid phase geochemical analyses from samples collected on R/V Savannah cruise SAV-16-16 at the Cape Lookout Continental Shelf and Slope during May 2016 (NCEI Accession 0278176)
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title: Sediment pore water and solid phase geochemical analyses from samples collected on R/V Savannah cruise SAV-16-16 at the Cape Lookout Continental Shelf and Slope during May 2016 (NCEI Accession 0278176)
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Anchor: http://lod.bco-dmo.org/id/person/743721 Martial Taillefert
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abstract: This dataset contains chemical data collected on R/V Savannah during cruise SAV-16-16 in the North Atlantic Ocean from 2016-05-17 to 2016-05-26. These data include dissolved inorganic Carbon, reactive phosphorus (PO4), and sulfate. The instruments used to collect these data include Flow Injection Analyzer, High Performance Liquid Chromatograph, Multi Corer, and Spectrophotometer. These data were collected by Martial Taillefert of Georgia Institute of Technology as part of the "Source, Composition, and Stability of Soluble Iron Fluxing from Continental Margin Sediments (Soluble Fe Fluxing)" project. The Biological and Chemical Oceanography Data Management Office (BCO-DMO) submitted these data to NCEI on 2020-03-19. The following is the text of the dataset description provided by BCO-DMO: Sediment pore water and solid phase geochemical analyses from samples collected on R/V Savannah cruise SAV-16-16 at the Cape Lookout Continental Shelf and Slope during May 2016 Dataset Description: Acquisition Description: Sediment cores were obtained by a MC-800 multi-corer and profiled immediately with voltammetric Hg/Au microelectrodes deployed on a computer-controlled micromanipulator (Beckler et al., 2016). Sediment pore waters were then extracted from the same core and either preserved until analysis or analyzed immediately onboard ship. Sampling and analyses were conducted immediately after sediment collection to minimize artifacts from exposure to the atmosphere. After profiling, sediments were immediately sliced under N₂ atmosphere and pore waters extracted by centrifugation at 3000 rpm under N₂ atmosphere. Finally, pore waters were immediately filtered (0.2 µM PSE Puradisc syringe filters, Whatman) under N₂ atmosphere and either preserved at -20C until analysis (SO₄²⁻), dispensed directly into reagents for analysis (SPO₄³⁻), or analyzed immediately (DIC). SO₄²⁻ was measured by non-suppressed HPLC with UV detection (Beckler et al., 2014). SPO₄³⁻ was measured spectrophotometrically using the molybdate-blue method after natural color correction to avoid interferences from dissolved silica and sulfides (Murphy and Riley, 1962). Finally, DIC was measured by flow injection analysis with conductivity detection after spiking samples with 10 mM ZnCl₂ to prevent dissolved sulfide interferences (Hall and Aller, 1992). All errors reported for the electrochemical measurements represent the standard deviation of at least triplicate measurements. Errors of all other parameters represent the analytical error propagated from calibration curves, dilution, and instrumental drift Problem report: Some of the data are missing because pore water volumes were too low to make all the measurements.
purpose: This dataset is available to the public for a wide variety of uses including scientific research and analysis.
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Anchor: https://www.nsf.gov/awardsearch/showAward?AWD_ID=1438648 Funding provided by NSF Division of Ocean Sciences (NSF OCE) Award Number: OCE-1438648 Award URL: http://www.nsf.gov/awardsearch/showAward.do?AwardNumber=1438648
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otherConstraints: Cite as: Taillefert, Martial (2023). Sediment pore water and solid phase geochemical analyses from samples collected on R/V Savannah cruise SAV-16-16 at the Cape Lookout Continental Shelf and Slope during May 2016 (NCEI Accession 0278176). [indicate subset used]. NOAA National Centers for Environmental Information. Dataset. https://www.ncei.noaa.gov/archive/accession/0278176. Accessed [date].
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title: Taillefert, M. (2020) Sediment pore water and solid phase geochemical analyses from samples collected on R/V Savannah cruise SAV-16-16 at the Cape Lookout Continental Shelf and Slope during May 2016. Biological and Chemical Oceanography Data Management Office (BCO-DMO). Dataset version 2020-03-17. https://doi.org/10.26008/1912/bco-dmo.806065.1
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beginPosition: 2016-05-17
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fees: In most cases, electronic downloads of the data are free. However, fees may apply for custom orders, data certifications, copies of analog materials, and data distribution on physical media.
orderingInstructions: Contact NCEI for other distribution options and instructions.
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description: automated chemical analysis instrument An instrument that performs flow injection analysis. Flow injection analysis (FIA) is an approach to chemical analysis that is accomplished by injecting a plug of sample into a flowing carrier stream. FIA is an automated method in which a sample is injected into a continuous flow of a carrier solution that mixes with other continuously flowing solutions before reaching a detector. Precision is dramatically increased when FIA is used instead of manual injections and as a result very specific FIA systems have been developed for a wide array of analytical techniques. https://www.bco-dmo.org/instrument/657 (accessed 2018-01-26) Laboratory instrument that analyzes multiple media for ions. The media include various solids and liquids. Models include: QuikChem 8000 Series FIA System
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description: spectrophotometer, optical spectrometer, spectrograph or spectroscope An optical spectrometer (spectrophotometer, spectrograph or spectroscope) is an instrument used to measure properties of light over a specific portion of the electromagnetic spectrum, typically used in spectroscopic analysis to identify materials. Butler, L. R. P.; Laqua, K. (1995). "Nomenclature, symbols, units and their usage in spectrochemical analysis-IX. Instrumentation for the spectral dispersion and isolation of optical radiation (IUPAC Recommendations 1995)". Pure Appl. Chem. IUPAC. 67 (10): 1725–1744. doi:10.1351/pac199567101725. A spectrometer is the general term for describing a combination of spectral apparatus with one or more detectors to measure the intensity of one or more spectral bands."
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description: R/V; commissioned 2001; Skidaway Institute of Oceanography; active July 2007
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